Synthesis of a magnetic polystyrene-supported Cu(II)-containing heterocyclic complex as a magnetically separable and reusable catalyst for the preparation of N-sulfonyl-N-aryl tetrazoles
| dc.contributor.author | Nasrollahzadeh, Mahmoud | |
| dc.contributor.author | Motahharifar, Narjes | |
| dc.contributor.author | Pakzad, Khatereh | |
| dc.contributor.author | Khorsandi, Zahra | |
| dc.contributor.author | Baran, Talat | |
| dc.contributor.author | Wang, Jinghan | |
| dc.contributor.author | Kruppke, Benjamin | |
| dc.contributor.author | Khonakdar, Hossein Ali | |
| dc.date.accessioned | 2023-02-27T07:51:50Z | |
| dc.date.available | 2023-02-27T07:51:50Z | |
| dc.date.issued | 2023 | |
| dc.department | Sabire Yazıcı Fen Edebiyat Fakültesi | |
| dc.description.abstract | In this work, a cost-effective, environmentally friendly, and convenient method for synthesizing a novel heterogeneous catalyst via modification of polystyrene using tetrazole-copper magnetic complex [Ps@Tet-Cu(II)@Fe3O4] has been successfully developed. The synthesized complex was analyzed using TEM (transmission electron microscopy), HRTEM (high resolution-transmission electron microscopy), STEM (scanning transmission electron microscopy), FFT (Fast Fourier transform), XRD (X-ray diffraction), FT-IR (Fourier transform-infrared spectroscopy), TG/DTG (Thermogravimetry and differential thermogravimetry), ICP-OES (Inductively coupled plasma-optical emission spectrometry), Vibrating sample magnetometer (VSM), EDS (energy dispersive X-ray spectroscopy), and elemental mapping. N-Sulfonyl-N-aryl tetrazoles were synthesized in high yields from N-sulfonyl-N-aryl cyanamides and sodium azide using Ps@Tet-Cu(II)@Fe3O4 nanocatalyst. The Ps@Tet-Cu(II)@Fe3O4 complex can be recycled and reused easily multiple times using an external magnet without significant loss of catalytic activity. | |
| dc.identifier.doi | 10.1038/s41598-023-30198-7 | |
| dc.identifier.issue | 1 | en_US |
| dc.identifier.pmid | 36828906 | |
| dc.identifier.scopusquality | Q1 | |
| dc.identifier.uri | https:/dx.doi.org/10.1038/s41598-023-30198-7 | |
| dc.identifier.uri | https://hdl.handle.net/20.500.12451/10302 | |
| dc.identifier.volume | 13 | en_US |
| dc.identifier.wos | WOS:000942280900053 | |
| dc.identifier.wosquality | Q1 | |
| dc.indekslendigikaynak | Web of Science | |
| dc.indekslendigikaynak | Scopus | |
| dc.indekslendigikaynak | PubMed | |
| dc.language.iso | en | |
| dc.publisher | Nature | |
| dc.relation.ispartof | Scientific Reports | |
| dc.relation.publicationcategory | Makale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı | |
| dc.rights | info:eu-repo/semantics/openAccess | |
| dc.subject | Synthesis of A Magnetic | |
| dc.subject | Polystyrene-supported Cu(II) | |
| dc.title | Synthesis of a magnetic polystyrene-supported Cu(II)-containing heterocyclic complex as a magnetically separable and reusable catalyst for the preparation of N-sulfonyl-N-aryl tetrazoles | |
| dc.type | Article |
