New fatty acid derivatives based on barbiturates and other cyclic beta-dicarbonyl compounds and an acyl migration

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dc.contributor.authorPesyan, Nader Noroozi
dc.contributor.authorBagheri, Marziyeh
dc.contributor.authorSahin, Ertan
dc.contributor.authorTunç, Tuncay
dc.date.accessioned13.07.201910:50:10
dc.date.accessioned2019-07-16T09:19:21Z
dc.date.available13.07.201910:50:10
dc.date.available2019-07-16T09:19:21Z
dc.date.issued2014
dc.departmentEğitim Fakültesi
dc.description.abstractThe use of DCC, triethylamine and 4-dimethylaminopyridine in dichloromethane provides a general and standard one-pot procedure for the O-acylation of cyclic beta-dicarbonyl compound derivatives (1) with palmitic and stearic acids which have long hydrocarbon tails, to synthesis of new type of fatty acid derivative in good to excellent yields. Structure elucidation was carried out by FT-IR, H-1 NMR and C-13 NMR spectroscopy techniques. The acyl migration was also found in results and the corresponding structure was characterized by X-ray crystallography. A proposed mechanism was discussed for the formation of products.
dc.description.sponsorshipResearch Council of Urmia University
dc.description.sponsorshipWe gratefully acknowledge financial support by the Research Council of Urmia University.
dc.identifier.doi10.1007/s13738-014-0415-9
dc.identifier.endpage1437en_US
dc.identifier.issn1735-207X
dc.identifier.issn1735-2428
dc.identifier.issue5en_US
dc.identifier.scopusqualityQ2
dc.identifier.startpage1429en_US
dc.identifier.urihttps://doi.org/10.1007/s13738-014-0415-9
dc.identifier.urihttps://hdl.handle.net/20.500.12451/4984
dc.identifier.volume11en_US
dc.identifier.wosWOS:000341185200023
dc.identifier.wosqualityN/A
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.language.isoen
dc.publisherSpringer
dc.relation.ispartofJournal of the Iranian Chemical Society
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.subjectBarbituric Acid
dc.subjectFatty Acid
dc.subject4-Dimethylaminopyridine
dc.subjectAcyl Migration
dc.subjectO-acylation
dc.titleNew fatty acid derivatives based on barbiturates and other cyclic beta-dicarbonyl compounds and an acyl migration
dc.typeArticle

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