Microwave assisted synthesis of biarlys by C-C coupling reactions with a new chitosan supported Pd(II) catalyst

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dc.authoridMENTES, AYFER -- 0000-0003-3946-4075; BARAN, TALAT -- 0000-0003-0206-3841
dc.contributor.authorBaran, Talat
dc.contributor.authorMenteş, Ayfer
dc.date.accessioned13.07.201910:50:10
dc.date.accessioned2019-07-29T19:26:51Z
dc.date.available13.07.201910:50:10
dc.date.available2019-07-29T19:26:51Z
dc.date.issued2016
dc.departmentFen-Edebiyat Fakültesi
dc.description.abstractIn this study a new type chitosan-based support has been produced for Pd(II) catalyst and its catalytic performance in Suzuki C-C reactions has been studied under microwave irradiation without using any solvent. The chemical identification of the catalyst was performed using TG/DTG, FTIR, UV-Vis ICP-OES, SEM/EDAX, C-13 NMR, molar conductivity, XRD and magnetic moment techniques. The performance of this new Pd(II) catalyst was studied in Suzuki C-C reactions. The Pd(II) catalyst exhibited a good catalytic performance in very short time (4 min) by giving high TONs and TOFs with low amount of the catalyst (0.015 mol%). The catalyst also had reusability and did not lose its activity until six runs.
dc.description.sponsorshipScientific and Technological Research Council of Turkey (TUBITAK) [113Z296]
dc.description.sponsorshipWe would like to thank the Scientific and Technological Research Council of Turkey (TUBITAK) (Project Number: 113Z296) for financial support.
dc.identifier.doi10.1016/j.molstruc.2016.05.091
dc.identifier.endpage116en_US
dc.identifier.issn0022-2860
dc.identifier.issn1872-8014
dc.identifier.scopusqualityQ1
dc.identifier.startpage111en_US
dc.identifier.urihttps://doi.org/10.1016/j.molstruc.2016.05.091
dc.identifier.urihttps://hdl.handle.net/20.500.12451/5726
dc.identifier.volume1122en_US
dc.identifier.wosWOS:000381167800013
dc.identifier.wosqualityN/A
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.language.isoen
dc.publisherELSEVIER SCIENCE BV
dc.relation.ispartofJOURNAL OF MOLECULAR STRUCTURE
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.subjectSuzuki C-C Reactions
dc.subjectChitosan
dc.subjectSchiff Base
dc.subjectReusability
dc.titleMicrowave assisted synthesis of biarlys by C-C coupling reactions with a new chitosan supported Pd(II) catalyst
dc.typeArticle

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