Fabrication of PAMP/Au and GO/PAMP/Au nanosensors for electrochemical detection of paracetamol in pharmaceutical preparations
| dc.contributor.author | Bilici, Ali | |
| dc.contributor.author | Denizhan, Nuray | |
| dc.contributor.author | Emre, Deniz | |
| dc.contributor.author | Soylukan, Caner | |
| dc.contributor.author | Algı, Fatih | |
| dc.contributor.author | Yılmaz, Selehattin | |
| dc.date.accessioned | 2021-12-08T06:26:25Z | |
| dc.date.available | 2021-12-08T06:26:25Z | |
| dc.date.issued | 2021 | |
| dc.department | Sabire Yazıcı Fen Edebiyat Fakültesi | |
| dc.description.abstract | This paper reports on the modification of Pencil Graphite Electrode (PGE) surface with the poly(2-amino-4-methylphenol)/gold (PAMP/Au) and graphene oxide/poly(2-amino-4-methylphenol)/gold (GO/PAMP/Au) nanocomposites, in two steps. The first step is based on the one-pot preparation of composites by template-free chemical oxidation process. In the second step, composites are deposited at PGE surface by electro-oxidation process. Both nanocomposites and modified PGE surfaces are characterized by X-Ray Diffraction method (XRD), Scanning Electron Microscopy (SEM), EDAX, and CV analyses. The electrochemical performances of modified electrodes (abbreviated as PAMP/Au-PGE and GO/PAMP/Au-PGE) were investigated. The limit of detection values for PGE, PAMP/Au-PGE, and GO/PAMP/Au-PGE were found to be 2.74 × 10–6, 5.29 × 10–7, and 2.91 × 10–8 mol/dm3, respectively. The limit of quantification values were determined as 9.14 × 10–6, 1.76 × 10–6, and 9.69 × 10–8 mol/dm3 for PGE, PAMP/Au-PGE, and GO/PAMP/Au-PGE, respectively. | |
| dc.identifier.doi | 10.1007/s00706-021-02866-9 | |
| dc.identifier.endpage | 1552 | en_US |
| dc.identifier.issn | 0026-9247 | |
| dc.identifier.issue | 12 | en_US |
| dc.identifier.scopusquality | Q2 | |
| dc.identifier.startpage | 1539 | en_US |
| dc.identifier.uri | https:/dx.doi.org/10.1007/s00706-021-02866-9 | |
| dc.identifier.uri | https://hdl.handle.net/20.500.12451/8894 | |
| dc.identifier.volume | 152 | en_US |
| dc.identifier.wos | WOS:000717903200001 | |
| dc.identifier.wosquality | Q4 | |
| dc.indekslendigikaynak | Web of Science | |
| dc.indekslendigikaynak | Scopus | |
| dc.language.iso | en | |
| dc.publisher | Springer | |
| dc.relation.ispartof | Monatshefte fur Chemie | |
| dc.relation.publicationcategory | Makale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı | |
| dc.rights | info:eu-repo/semantics/embargoedAccess | |
| dc.subject | Electrochemistry | |
| dc.subject | Graphene Oxide | |
| dc.subject | Pencil Graphite Electrode | |
| dc.subject | Poly(2-hydroxy-5-methylaniline) | |
| dc.subject | Polymerization | |
| dc.subject | Sensors | |
| dc.title | Fabrication of PAMP/Au and GO/PAMP/Au nanosensors for electrochemical detection of paracetamol in pharmaceutical preparations | |
| dc.type | Article |
