Synthesis, crystal structure, and spectroscopic studies of n-(4-bromobenzylidene)-n '-(2-pyridyl) hydrazine schiff base molecule

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dc.authoridFen Bilgisi Egitimi, Aksaray Egitim -- 0000-0001-8976-571X; Tunc, Tuncay -- 0000-0002-3576-2633; Ozcelik, Nefise -- 0000-0002-6972-1071
dc.contributor.authorTunç, Tuncay
dc.contributor.authorTezcan, Habibe
dc.contributor.authorŞahin, Ertan
dc.contributor.authorDilek, Nefise
dc.date.accessioned13.07.201910:50:10
dc.date.accessioned2019-07-29T19:28:09Z
dc.date.available13.07.201910:50:10
dc.date.available2019-07-29T19:28:09Z
dc.date.issued2012
dc.departmentEğitim Fakültesi
dc.description.abstractA new Schiff base complex N-(4-bromobenzylidene)-N'-(2-pyridyl) hydrazine, C12H10N3Br, has been synthesized and characterized by elemental analyses, mass, H-1 NMR, ultraviolet-visible (UV-VIS), and IR spectroscopy and single-crystal X-ray determination. The p-Br-benzene and pyridine rings are almost planar and the dihedral angle between the planes is 11.1(3)degrees. The crystal structure is stabilized by intermolecular N-H center dot center dot center dot N-Py hydrogen bonding interaction. X-ray diffraction analyses show that N-(4-bromobenzylidene)-N'-(2-pyridyl) hydrazine Schiff base molecule crystallizes in the monoclinic system, P2(1)/c space group, a = 5.611(5) angstrom, b = 19.566(5) angstrom, c = 10.715(5) angstrom, beta = 98.766(5)degrees, and V = 1162.60(12) angstrom(3).
dc.identifier.doi10.1080/15421406.2011.591702
dc.identifier.endpage208en_US
dc.identifier.issn1542-1406
dc.identifier.issn1563-5287
dc.identifier.scopusqualityQ4
dc.identifier.startpage194en_US
dc.identifier.urihttps://doi.org/10.1080/15421406.2011.591702
dc.identifier.urihttps://hdl.handle.net/20.500.12451/5995
dc.identifier.volume552en_US
dc.identifier.wosWOS:000302297400018
dc.identifier.wosqualityN/A
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.language.isoen
dc.publisherTaylor & Francis Ltd
dc.relation.ispartofMolecular Crystals and Liquid Crystals
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/embargoedAccess
dc.subjectCondensation Reaction
dc.subjectCrystal Structure
dc.subjectHydrazone
dc.subjectSchiff Base
dc.subjectX-ray Diffraction
dc.titleSynthesis, crystal structure, and spectroscopic studies of n-(4-bromobenzylidene)-n '-(2-pyridyl) hydrazine schiff base molecule
dc.typeArticle

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