Synthesis and characterization of novel chiral (1r,2r)-1,2-bis[5-(aminomethylphospinic acid)-1,3,4-thiadiazol-2-yl]ethane-1,2-diols

Basit Öğe Kaydı
dc.authoridorek, cahit -- 0000-0002-3854-1537
dc.contributor.authorKoparir, Pelin
dc.contributor.authorKaraarslan, Muhsin
dc.contributor.authorÖrek, Cahit
dc.contributor.authorKoparır, Metin
dc.date.accessioned13.07.201910:50:10
dc.date.accessioned2019-07-16T09:15:56Z
dc.date.available13.07.201910:50:10
dc.date.available2019-07-16T09:15:56Z
dc.date.issued2012
dc.departmentSabire Yazıcı Fen Edebiyat Fakültesi
dc.description.abstract(1R,2R)-1,2-bis[5-(arylideneamino)-1,3,4-thiadiazol-2-yl]ethane-1,2-diol (2a-d) were synthesized by using appropriate aldehydes and (1R,2R)-1,2-bis(5-amino-1,3,4-thiadiazol-2-yl)ethane-1,2-diol (1) as a starting compound. Then, the phosphinic acid component (3a-d) were obtained from (2a-d) and hypophosporus acid. In addition, the structures of the novel chiral compounds (2a-d) and (3a-d) were confirmed by elemental analyses, IR, H-1-NMR, C-13-NMR, and P-31-NMR spectra. H-1 NMR and C-13 NMR spectra for 1, 2a, and 3a (Figures S1-S6) are available online in the Supplemental Materials.
dc.description.sponsorshipFirat University (FUBAP) [FF.11.17]
dc.description.sponsorshipThis work was supported by Grant no. FF.11.17 of the Research Fund of Firat University (FUBAP).
dc.identifier.doi10.1080/10426507.2011.636412
dc.identifier.endpage870en_US
dc.identifier.issn1042-6507
dc.identifier.issn1563-5325
dc.identifier.issue7en_US
dc.identifier.scopusqualityQ3
dc.identifier.startpage864en_US
dc.identifier.urihttps://doi.org/10.1080/10426507.2011.636412
dc.identifier.urihttps://hdl.handle.net/20.500.12451/4498
dc.identifier.volume187en_US
dc.identifier.wosWOS:000304595400008
dc.identifier.wosqualityN/A
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.language.isoen
dc.publisherTaylor & Francis Ltd
dc.relation.ispartofPhosphorus Sulfur and Silicon and the Related Elements
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/embargoedAccess
dc.subject1,3,4-Thiadiazole
dc.subjectAminophosphinic Acid
dc.subjectTartaric Acid
dc.subjectEthane-1,2-diol
dc.titleSynthesis and characterization of novel chiral (1r,2r)-1,2-bis[5-(aminomethylphospinic acid)-1,3,4-thiadiazol-2-yl]ethane-1,2-diols
dc.typeArticle

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