Synthesis and characterization of boron-doped hafnia electrospun nanofibers and nanocrystalline ceramics

dc.authoridFen Bilgisi Egitimi, Aksaray Egitim -- 0000-0001-8976-571X; Tunc, Tuncay -- 0000-0002-3576-2633; Aytimur, Arda -- 0000-0001-6995-6164
dc.contributor.authorUslu, İbrahim
dc.contributor.authorTunç, Tuncay
dc.contributor.authorÖztürk, Mustafa Kemal
dc.contributor.authorAytimur, A.
dc.date.accessioned13.07.201910:50:10
dc.date.accessioned2019-07-29T19:26:40Z
dc.date.available13.07.201910:50:10
dc.date.available2019-07-29T19:26:40Z
dc.date.issued2012
dc.departmentEğitim Fakültesi
dc.description.abstractIn this study, boron-doped poly(vinyl) alcohol/HfO2 nanofibers were prepared by electrospinning using PVA as a precursor. The effect of boron doping was investigated in terms of solution properties, morphological changes and thermal characteristics. Nanofiber mats were calcined first at 800 degrees C. Then, the calcined products were pelleted and sintered at a rate of 8 degrees C/min and remained 2 h at 850 degrees C at atmospheric conditions to produce ultrafine ceramic nanocrystalline powders. The fibers and nanocrystalline powders were characterized by FT-IR, XPS, XRD and SEM. The addition of boron did not only increase the thermal stability of the fibers, but also their diameters, which yielded stronger fibers. The addition of boron did not only increase the thermal stability of the fibers, but also their diameters, which yielded stronger fibers.
dc.identifier.doi10.1080/03602559.2011.625383
dc.identifier.endpage262en_US
dc.identifier.issn0360-2559
dc.identifier.issue3en_US
dc.identifier.scopusqualityN/A
dc.identifier.startpage257en_US
dc.identifier.urihttps://doi.org/10.1080/03602559.2011.625383
dc.identifier.urihttps://hdl.handle.net/20.500.12451/5675
dc.identifier.volume51en_US
dc.identifier.wosWOS:000302367400007
dc.identifier.wosqualityN/A
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.language.isoen
dc.publisherTaylor & Francis
dc.relation.ispartofPolymer - Plastics Technology and Engineering
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/closedAccess
dc.subjectBoric Acid
dc.subjectElectrospinning
dc.subjectHafnia
dc.subjectNanofibers
dc.subjectPoly(vinyl) Alcohol
dc.titleSynthesis and characterization of boron-doped hafnia electrospun nanofibers and nanocrystalline ceramics
dc.typeArticle

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