4-Hydroxy-N'-[(1E)-1-(4-methylphenyl)ethylidene]benzohydrazide: Synthesis, crystal structure, and spectroscopic studies

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dc.authoridGUNES, Prof. Dr. Bilal -- 0000-0002-3911-6778; Ozcelik, Nefise -- 0000-0002-6972-1071; Gokce, Cansu -- 0000-0002-6834-4841
dc.contributor.authorDilek, Nefise
dc.contributor.authorGüneş, Bilal
dc.contributor.authorGökçe, Cansu
dc.contributor.authorGüp, Ramazan
dc.date.accessioned13.07.201910:50:10
dc.date.accessioned2019-07-16T09:19:42Z
dc.date.available13.07.201910:50:10
dc.date.available2019-07-16T09:19:42Z
dc.date.issued2013
dc.department[Dilek, N.] Aksaray Univ, Dept Phys, Arts & Sci Fac, TR-68100 Aksaray, Turkey -- [Gunes, B.] Gazi Univ, Gazi Educ Fac, Dept Phys Educ, TR-06500 Ankara, Turkey -- [Gokce, C. -- Gup, R.] Mugla Univ, Arts & Sci Fac, Dept Chem, TR-48000 Kotekli, Mugla, Turkey
dc.description.abstractThe titled compound has been synthesized by reaction of 4'-methylacetophenon with 4-hydrox-ybenzohydrazide in presence of catalytic amount of glacial acetic acid. The compound is characterized by elemental analysis, IR, H-1 NMR, C-13 NMR and UV-visible spectra. The crystal structure was determined by X-ray diffraction method. Both X-ray data and NMR spectra indicate that the molecule exists in a trans configuration with respect to the C=N bond. The observation of strong nu(C=O) peak in IR spectra of the aroylhydrazone compound suggests that it is in keto form in solid state. X-ray diffraction results confirm this suggestion. In the crystal structure, there are N-H...O and O-H...O hydrogen bonds and weak C-H...pi interaction.
dc.identifier.doi10.1134/S1063774513080026
dc.identifier.endpage1078en_US
dc.identifier.issn1063-7745
dc.identifier.issn1562-689X
dc.identifier.issue7en_US
dc.identifier.scopusqualityQ4
dc.identifier.startpage1073en_US
dc.identifier.urihttps://doi.org/10.1134/S1063774513080026
dc.identifier.urihttps://hdl.handle.net/20.500.12451/5022
dc.identifier.volume58en_US
dc.identifier.wosWOS:000329101900022
dc.identifier.wosqualityN/A
dc.indekslendigikaynakWeb of Science
dc.indekslendigikaynakScopus
dc.language.isoen
dc.publisherMAIK NAUKA/INTERPERIODICA/SPRINGER
dc.relation.ispartofCRYSTALLOGRAPHY REPORTS
dc.relation.publicationcategoryMakale - Uluslararası Hakemli Dergi - Kurum Öğretim Elemanı
dc.rightsinfo:eu-repo/semantics/openAccess
dc.title4-Hydroxy-N'-[(1E)-1-(4-methylphenyl)ethylidene]benzohydrazide: Synthesis, crystal structure, and spectroscopic studies
dc.typeArticle

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