Crystal structure of bis(isothiocyanato)[2,6-diacetylpyridine bis(4-hydroxybenzoylhydrazone)]Fe(III) chloride bis(dimethylformamide) solvate

Dilek, NefiseGüneş, BilalBüyükgüngör, OrhanGüp, Ramazan13.07.20192019-07-2913.07.20192019-07-2920131063-7745https://doi.org/10.1134/S1063774513010173https://hdl.handle.net/20.500.12451/6193The crystal structure of title compound (Fe[(C25H21N7O4S2)] center dot 4(C3NOH7), where C3NOH7 is dimethylformamide, DMF) was determined by the X-ray diffraction method. This compound crystallizes in the monoclinic C2/c space group, Z = 4. Unit cell parameters are: a = 13.6080(5), b = 17.6375(7), c = 19.5571(6) , beta = 108.753(2)A degrees. The N-H...O and O-H...O interactions stabilize the molecules in the lattice. The structure contains also the solvent dimethylformamide molecules, which are connected with intermoleculer hydrogen bond. The O atoms of DMF molecules take place as acceptor atoms.eninfo:eu-repo/semantics/closedAccessCrystal structure of bis(isothiocyanato)[2,6-diacetylpyridine bis(4-hydroxybenzoylhydrazone)]Fe(III) chloride bis(dimethylformamide) solvateArticle5819810110.1134/S1063774513010173Q4WOS:000314065700011N/A